5YP6

RORgamma (263-509) complexed with SRC2 and Compound 6

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U1
Synchrotron site	SSRF
Beamline	BL17U1
Temperature [K]	90
Detector technology	CCD
Collection date	2010-11-24
Detector	MARMOSAIC 225 mm CCD
Wavelength(s)	0.9792
Spacegroup name	P 41 21 2
Unit cell lengths	62.201, 62.201, 154.822
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	57.720 - 2.200
R-factor	0.21464
Rwork	0.213
R-free	0.25446
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	3l0j
RMSD bond length	0.005
RMSD bond angle	0.820
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	REFMAC (5.5.0102)

Data quality characteristics

	Overall
Low resolution limit [Å]	57.720
High resolution limit [Å]	2.200
Number of reflections	15356
<I/σ(I)>	24.19
Completeness [%]	100.0
Redundancy	12.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	6.5	293	0.2M Ammonium Sulfate, 0.1M Bis-Tris, pH 6.5, 14%(w/v) PEG 8000