5YOU

Crystal structure of BRD4-BD1 bound with hjp64

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U1
Synchrotron site	SSRF
Beamline	BL17U1
Temperature [K]	100
Detector technology	CCD
Collection date	2015-12-17
Detector	ADSC QUANTUM 315r
Wavelength(s)	0.97923
Spacegroup name	P 21 21 21
Unit cell lengths	34.622, 47.598, 77.954
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	40.624 - 1.503
R-factor	0.2098
Rwork	0.208
R-free	0.24820
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.006
RMSD bond angle	0.821
Data scaling software	XDS
Phasing software	PHASER
Refinement software	PHENIX ((1.11_2567: ???))

Data quality characteristics

	Overall
Low resolution limit [Å]	47.598
High resolution limit [Å]	1.503
Number of reflections	18473
<I/σ(I)>	17.5
Completeness [%]	87.2
Redundancy	5.75

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	3.6M Naformate, 10% glycerol