5YM6
Crystal Structure of porcine delta coronavirus nsp9
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL17U1 |
| Synchrotron site | SSRF |
| Beamline | BL17U1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2016-09-19 |
| Detector | ADSC QUANTUM 315 |
| Wavelength(s) | 0.97917 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 57.969, 55.185, 69.445 |
| Unit cell angles | 90.00, 90.01, 90.00 |
Refinement procedure
| Resolution | 29.789 - 1.803 |
| R-factor | 0.2082 |
| Rwork | 0.206 |
| R-free | 0.24580 |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.018 |
| Data reduction software | HKL-3000 |
| Data scaling software | HKL-3000 |
| Phasing software | PHENIX |
| Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 1.800 |
| Number of reflections | 40635 |
| <I/σ(I)> | 15.71 |
| Completeness [%] | 97.4 |
| Redundancy | 3.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 3.5 | 293 | 3.0 M sodium chloride, 0.1 M citric acid (pH 3.5) |
