5YAH
Crystal 2 for AtLURE1.2-AtPRK6LRR
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-07-12 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.0 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 98.706, 43.347, 77.821 |
Unit cell angles | 90.00, 124.70, 90.00 |
Refinement procedure
Resolution | 31.992 - 2.104 |
R-factor | 0.226 |
Rwork | 0.224 |
R-free | 0.26580 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.225 |
Data reduction software | DENZO |
Data scaling software | HKL-3000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.8_1069) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 31.992 | 2.240 |
High resolution limit [Å] | 2.104 | 2.104 |
Number of reflections | 15868 | |
<I/σ(I)> | 30.5 | |
Completeness [%] | 99.7 | |
Redundancy | 4.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291 | MgCl2, Bis-Tris pH 5.5, PEG 3350 |