5XVR

EarP bound with dTDP-rhamnose (co-crystal)

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SPRING-8 BEAMLINE BL41XU
Synchrotron site	SPring-8
Beamline	BL41XU
Temperature [K]	90
Detector technology	PIXEL
Collection date	2017-05-24
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	1
Spacegroup name	P 21 21 2
Unit cell lengths	97.390, 195.190, 46.320
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	48.798 - 1.630
R-factor	0.1652
Rwork	0.164
R-free	0.19990
Structure solution method	FOURIER SYNTHESIS
RMSD bond length	0.011
RMSD bond angle	1.120
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	PHENIX
Refinement software	PHENIX ((1.11.1_2575: ???))

Data quality characteristics

	Overall
Low resolution limit [Å]	48.800
High resolution limit [Å]	1.630
Number of reflections	110150
<I/σ(I)>	19.7
Completeness [%]	99.1
Redundancy	21.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		277	8% tacsimate pH 6.0, 12% PEG6000, 0.2M lithium sulfate, 10mM dTDP-rhamnose