5XP5

C-Src in complex with ATP-Chf

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 5.0.2
Synchrotron site	ALS
Beamline	5.0.2
Temperature [K]	80
Detector technology	CCD
Collection date	2014-01-01
Detector	ADSC QUANTUM 315r
Wavelength(s)	0.987
Spacegroup name	P 1
Unit cell lengths	42.288, 63.687, 73.815
Unit cell angles	79.07, 89.23, 89.24

Refinement procedure

Resolution	43.446 - 2.101
R-factor	0.2191
Rwork	0.218
R-free	0.24620
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	4u5j
RMSD bond length	0.004
RMSD bond angle	0.854
Refinement software	PHENIX (1.8.4_1496)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	43.500	2.110
High resolution limit [Å]	2.100	2.070
Rpim	0.057
Number of reflections	41453	299
<I/σ(I)>	15.18
Completeness [%]	94.1
Redundancy	10	1.8
CC(1/2)		0.313

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		291	PEG 4000