5XI4

BRD4 bound with compound Bdi4

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U1
Synchrotron site	SSRF
Beamline	BL17U1
Temperature [K]	100
Detector technology	CCD
Collection date	2016-12-02
Detector	ADSC QUANTUM 315r
Wavelength(s)	0.9792
Spacegroup name	P 21 21 21
Unit cell lengths	35.124, 47.421, 77.817
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	32.010 - 1.486
R-factor	0.2188
Rwork	0.217
R-free	0.25320
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.008
RMSD bond angle	0.961
Data reduction software	XDS
Data scaling software	XDS
Refinement software	PHENIX ((1.11_2567: ???))

Data quality characteristics

	Overall
Low resolution limit [Å]	32.010
High resolution limit [Å]	1.486
Number of reflections	20854
<I/σ(I)>	15.97
Completeness [%]	94.4
Redundancy	2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	2.3 M NAFORMATE, 10% GLYCEROL