5XG7

Galectin-13/Placental Protein 13 crystal structure

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL18U1
Synchrotron site	SSRF
Beamline	BL18U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2016-10-21
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.9
Spacegroup name	C 2 2 2
Unit cell lengths	57.879, 92.104, 50.752
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	19.080 - 1.550
R-factor	0.1622
Rwork	0.159
R-free	0.18730
Structure solution method	MOLECULAR REPLACEMENT
Refinement software	REFMAC

Data quality characteristics

	Overall
Low resolution limit [Å]	19.080
High resolution limit [Å]	1.550
Rmerge	0.081
Number of reflections	19963
<I/σ(I)>	13.6
Completeness [%]	95.6
Redundancy	6.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	EVAPORATION		298	PEG