5XAE
mutNLIR_LC3B
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE AR-NE3A |
Synchrotron site | Photon Factory |
Beamline | AR-NE3A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-03-18 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 |
Unit cell lengths | 41.720, 53.447, 61.584 |
Unit cell angles | 77.15, 73.18, 85.05 |
Refinement procedure
Resolution | 39.923 - 1.996 |
R-factor | 0.2224 |
Rwork | 0.220 |
R-free | 0.25870 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3vtu |
RMSD bond length | 0.012 |
RMSD bond angle | 1.727 |
Data reduction software | DENZO |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.11.1_2575)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 39.923 |
High resolution limit [Å] | 1.996 |
Number of reflections | 32311 |
<I/σ(I)> | 19.78 |
Completeness [%] | 95.7 |
Redundancy | 2.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293 | Pentaerythritol propoxylate, 0.1M HEPES pH 7.0, 0.2M Potassium chloride. |