5X3O
Crystal structure of p-DiUb-S65-COOH
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU MICROMAX-007 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2016-12-26 |
| Detector | DECTRIS PILATUS 200K |
| Wavelength(s) | 1.54 |
| Spacegroup name | P 1 2 1 |
| Unit cell lengths | 40.608, 33.764, 44.686 |
| Unit cell angles | 90.00, 103.49, 90.00 |
Refinement procedure
| Resolution | 43.453 - 2.194 |
| R-factor | 0.2445 |
| Rwork | 0.240 |
| R-free | 0.31530 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.089 |
| Data reduction software | HKL-3000 |
| Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 43.453 |
| High resolution limit [Å] | 2.194 |
| Number of reflections | 6127 |
| <I/σ(I)> | 2.53 |
| Completeness [%] | 98.5 |
| Redundancy | 6.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 289 | 0.2M Ammonium phosphate monobasic, 20%(w/v) Polyethylene glycol 3350 |
