5X3N
Crystal structure of DiUb-K6
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-01-09 |
Detector | DECTRIS PILATUS 200K |
Wavelength(s) | 1.54 |
Spacegroup name | P -1 |
Unit cell lengths | 26.048, 26.278, 46.193 |
Unit cell angles | 102.05, 94.14, 99.63 |
Refinement procedure
Resolution | 44.896 - 1.649 |
R-factor | 0.219 |
Rwork | 0.216 |
R-free | 0.27590 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 0.832 |
Data reduction software | HKL-3000 |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 44.896 |
High resolution limit [Å] | 1.649 |
Number of reflections | 11102 |
<I/σ(I)> | 2.35 |
Completeness [%] | 78.5 |
Redundancy | 3.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 289 | 0.2M Magnesium formate dihydrate, 20%(w/v) Polyethylene glycol 3350 |