5WY3
Crystal structure of Chaetomium thermophilum Utp10 middle domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-06-30 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97853 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 91.052, 91.052, 554.758 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.947 - 3.200 |
R-factor | 0.2259 |
Rwork | 0.222 |
R-free | 0.26570 |
Structure solution method | SAD |
RMSD bond length | 0.011 |
RMSD bond angle | 1.397 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.11rc1_2513: ???)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 19.947 | 19.947 | 3.390 |
High resolution limit [Å] | 3.200 | 8.740 | 3.200 |
Rmerge | 0.101 | 0.043 | 1.189 |
Rmeas | 0.103 | 0.044 | 1.220 |
Number of reflections | 23700 | 1916 | 6682 |
<I/σ(I)> | 21.1 | 72.87 | 2.66 |
Completeness [%] | 99.2 | 91.5 | 99.1 |
Redundancy | 20.753 | ||
CC(1/2) | 1.000 | 0.999 | 0.919 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.1 M Hepes-Na, 2.0 M ammonium sulfate |