5WVC

Structure of the CARD-CARD disk

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	NSRRC BEAMLINE BL13B1
Synchrotron site	NSRRC
Beamline	BL13B1
Temperature [K]	93
Detector technology	CCD
Collection date	2014-08-08
Detector	ADSC QUANTUM 315
Wavelength(s)	1.0000
Spacegroup name	P 61
Unit cell lengths	190.110, 190.110, 68.828
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	24.852 - 2.993
R-factor	0.1992
Rwork	0.197
R-free	0.22810
RMSD bond length	0.003
RMSD bond angle	0.672
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHENIX
Refinement software	PHENIX (1.9_1692)

Data quality characteristics

	Overall
Low resolution limit [Å]	24.852
High resolution limit [Å]	2.993
Number of reflections	28208
<I/σ(I)>	6.8
Completeness [%]	97.7
Redundancy	2.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		298	0.2 M NH4I, 20% PEG 3350