5WK3
CRYSTAL STRUCTURE OF THE COMPLEX BETWEEN CCL17 AND M116 FAB
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2012-06-23 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 1.0 |
| Spacegroup name | P 1 |
| Unit cell lengths | 51.510, 81.930, 130.500 |
| Unit cell angles | 93.96, 99.21, 104.19 |
Refinement procedure
| Resolution | 15.000 - 1.900 |
| R-factor | 0.18094 |
| Rwork | 0.180 |
| R-free | 0.23147 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1nr4 |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.255 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 1.950 |
| High resolution limit [Å] | 1.900 | 1.900 |
| Rmerge | 0.075 | 0.480 |
| Number of reflections | 153743 | 10386 |
| <I/σ(I)> | 9.3 | 2.3 |
| Completeness [%] | 96.2 | 87.9 |
| Redundancy | 2.7 | 2.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7.4 | 293 | 15% PEG 3350, 0.2 M POTASSIUM SODIUM TARTRATE |
