5WHV
Crystal structure of ArtB
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2014-08-21 |
| Detector | RIGAKU SATURN 944 |
| Wavelength(s) | 1.5418 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 140.872, 94.231, 125.230 |
| Unit cell angles | 90.00, 103.62, 90.00 |
Refinement procedure
| Resolution | 31.124 - 2.303 |
| R-factor | 0.169 |
| Rwork | 0.167 |
| R-free | 0.21300 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4rhr |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.189 |
| Data scaling software | HKL-2000 |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.8.1_1168) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 2.300 |
| Number of reflections | 68092 |
| <I/σ(I)> | 17.42 |
| Completeness [%] | 96.6 |
| Redundancy | 3.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 297 | peg 200, calcium chloride |
