5WGP
Human Carbonic Anhydrase IX-mimic complexed with AceK
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | CHESS BEAMLINE F1 |
| Synchrotron site | CHESS |
| Beamline | F1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2016-05-16 |
| Detector | DECTRIS PILATUS3 6M |
| Wavelength(s) | 0.9770 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 41.819, 41.108, 72.023 |
| Unit cell angles | 90.00, 103.88, 90.00 |
Refinement procedure
| Resolution | 40.598 - 1.530 |
| R-factor | 0.1658 |
| Rwork | 0.165 |
| R-free | 0.18980 |
| RMSD bond length | 0.005 |
| RMSD bond angle | 0.873 |
| Data scaling software | SCALEPACK |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.10pre_2097) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 40.600 |
| High resolution limit [Å] | 1.530 |
| Number of reflections | 55129 |
| <I/σ(I)> | 15.9 |
| Completeness [%] | 99.6 |
| Redundancy | 3.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 298 | 1.6 M sodium citrate, 50 mM Tris |
