5W2W
INFLUENZA VIRUS NEURAMINIDASE N9 IN COMPLEX WITH 8-DEOXYGENATED 2,3-DIFLUORO-N-ACETYLNEURAMINIC ACID
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX1 |
Synchrotron site | Australian Synchrotron |
Beamline | MX1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-08-15 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 0.953242 |
Spacegroup name | I 4 3 2 |
Unit cell lengths | 180.709, 180.709, 180.709 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.300 - 1.850 |
R-factor | 0.142 |
Rwork | 0.140 |
R-free | 0.17100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4weg |
RMSD bond length | 0.019 |
RMSD bond angle | 1.977 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0155) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.300 | 1.850 |
High resolution limit [Å] | 1.850 | 1.800 |
Rmerge | 0.297 | 0.820 |
Number of reflections | 40605 | |
<I/σ(I)> | 10 | 1.2 |
Completeness [%] | 99.8 | 99 |
Redundancy | 75 | 29 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.7 | 298 | 1.7M POTASSIUM PHOSPHATE |