5VO4
Crystal Structure Of The Androgen Receptor Ligand Binding Domain In Complex With 5-(2-fluoro-4-hydroxyphenyl)-1-methyl-1H-pyrrole-2-carbonitrile
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU FR-D |
| Temperature [K] | 288 |
| Detector technology | CCD |
| Collection date | 2009-10-10 |
| Detector | RIGAKU SATURN 92 |
| Wavelength(s) | 1.54 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 55.123, 66.136, 70.183 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 36.260 - 2.350 |
| R-factor | 0.22862 |
| Rwork | 0.226 |
| R-free | 0.28230 |
| RMSD bond length | 0.008 |
| RMSD bond angle | 0.971 |
| Data reduction software | DENZO |
| Data scaling software | DENZO |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.5.0072) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 36.260 |
| High resolution limit [Å] | 2.350 |
| Number of reflections | 11169 |
| <I/σ(I)> | 25 |
| Completeness [%] | 99.5 |
| Redundancy | 3.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 300 | 30% PEG400, HEPES pH 7, 200mM Ca Cl |
