5VLG

Crystal structure of EilR in complex with malachite green

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 8.2.2
Synchrotron site	ALS
Beamline	8.2.2
Temperature [K]	100
Detector technology	AREA DETECTOR
Collection date	2014-10-14
Detector	ADSC QUANTUM 315r
Wavelength(s)	1.0000
Spacegroup name	P 1 21 1
Unit cell lengths	100.145, 85.985, 102.275
Unit cell angles	90.00, 101.69, 90.00

Refinement procedure

Resolution	50.076 - 2.932
R-factor	0.199
Rwork	0.197
R-free	0.24010
RMSD bond length	0.002
RMSD bond angle	0.468
Data reduction software	xia2
Data scaling software	xia2
Phasing software	PHASER
Refinement software	PHENIX ((dev_2650: ???))

Data quality characteristics

	Overall
Low resolution limit [Å]	50.076
High resolution limit [Å]	2.930
Number of reflections	36135
<I/σ(I)>	6.8
Completeness [%]	99.9
Redundancy	2.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	0.2 M Tri-Sodium citrate, 20 % PEG 3350