5VIZ
X-Ray structure of Insulin Glargine
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALBA BEAMLINE XALOC |
Synchrotron site | ALBA |
Beamline | XALOC |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-07-06 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.951 |
Spacegroup name | I 21 3 |
Unit cell lengths | 77.997, 77.997, 77.997 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 55.150 - 1.700 |
R-factor | 0.1642 |
Rwork | 0.162 |
R-free | 0.18260 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.028 |
RMSD bond angle | 2.236 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0103) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 55.160 |
High resolution limit [Å] | 1.700 |
Number of reflections | 8880 |
<I/σ(I)> | 21.5 |
Completeness [%] | 99.8 |
Redundancy | 6.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | BATCH MODE | 291 | Microbatch |