5V76
Structure of Haliangium ochraceum BMC-T HO-3341
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.2 |
Synchrotron site | ALS |
Beamline | 5.0.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-04-30 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.000 |
Spacegroup name | P 21 3 |
Unit cell lengths | 110.571, 110.571, 110.571 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.090 - 1.550 |
R-factor | 0.1577 |
Rwork | 0.157 |
R-free | 0.17090 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4ht5 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.094 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((dev_2650)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.090 | 1.630 |
High resolution limit [Å] | 1.550 | 1.550 |
Rmerge | 0.103 | 1.797 |
Number of reflections | 65376 | 9459 |
<I/σ(I)> | 26.9 | 2.6 |
Completeness [%] | 99.9 | 100 |
Redundancy | 42.6 | 44 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 295 | 0.1M cacodylate pH 6.5 1.25M citrate |