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5USZ

JAK2 JH2 in complex with JNJ-7706621

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU MICROMAX-007 HF
Temperature [K]100
Detector technologyPIXEL
Collection date2015-03-04
DetectorDECTRIS PILATUS 200K
Wavelength(s)1.54
Spacegroup nameP 1 21 1
Unit cell lengths44.716, 57.533, 60.769
Unit cell angles90.00, 110.41, 90.00
Refinement procedure
Resolution41.910 - 2.103
R-factor0.1744
Rwork0.172
R-free0.22350
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)4fvp
RMSD bond length0.002
RMSD bond angle0.580
Data reduction softwareHKL-2000
Data scaling softwareSCALEPACK
Phasing softwarePHASER
Refinement softwarePHENIX (1.11.1_2575)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]41.910
High resolution limit [Å]2.1002.100
Number of reflections16371
<I/σ(I)>9.6
Completeness [%]96.7
Redundancy3.2
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP82770.1M Tris, pH 8.0 0.2M Sodium acetate 12-20% PEG 4,000

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