5UE3
proMMP-9desFnII
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID23-1 |
| Synchrotron site | ESRF |
| Beamline | ID23-1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2007-03-05 |
| Detector | ADSC QUANTUM 315 |
| Wavelength(s) | 1 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 90.300, 73.200, 77.500 |
| Unit cell angles | 90.00, 106.30, 90.00 |
Refinement procedure
| Resolution | 32.840 - 1.599 |
| R-factor | 0.1575 |
| Rwork | 0.154 |
| R-free | 0.18380 |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.240 |
| Data reduction software | d*TREK |
| Refinement software | PHENIX ((1.10_2155: ???)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 49.190 |
| High resolution limit [Å] | 1.599 |
| Rmerge | 0.048 |
| Number of reflections | 62722 |
| <I/σ(I)> | 13.4 |
| Completeness [%] | 98.1 |
| Redundancy | 3.19 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 5.5 | 293 | 25% PEG 8K 1% glycerol 0.2 M ammonium sulfate 100 mM NaCacodylate |
