5TUR

Pim-1 kinase in complex with a 7-azaindole

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 21-ID-F
Synchrotron site	APS
Beamline	21-ID-F
Temperature [K]	100
Detector technology	CCD
Collection date	2007-02-01
Detector	MARMOSAIC 225 mm CCD
Wavelength(s)	1.00
Spacegroup name	P 65
Unit cell lengths	97.747, 97.747, 80.792
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	37.492 - 2.948
R-factor	0.2087
Rwork	0.204
R-free	0.24780
RMSD bond length	0.002
RMSD bond angle	0.668
Refinement software	PHENIX ((1.11_2567: ???))

Data quality characteristics

	Overall
Low resolution limit [Å]	37.492
High resolution limit [Å]	2.948
Number of reflections	9343
<I/σ(I)>	2.69
Completeness [%]	99.8
Redundancy	13

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION		277	0.1M imidazole, 1M NaAcetate, 20% glycerol pH 6.5