5TIQ

The Structure of the Major Capsid protein of PBCV-1

Replaces:  1J5Q

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 14-ID-B
Synchrotron site	APS
Beamline	14-ID-B
Temperature [K]	100
Detector technology	CCD
Collection date	2001-11-14
Detector	ADSC QUANTUM 4
Wavelength(s)	1.0069
Spacegroup name	P 41 3 2
Unit cell lengths	188.763, 188.763, 188.763
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	43.305 - 2.537
R-factor	0.1806
Rwork	0.179
R-free	0.22300
RMSD bond length	0.003
RMSD bond angle	0.925
Refinement software	PHENIX ((1.12_2829: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	84.420	2.640
High resolution limit [Å]	2.540	2.540
Rmerge	0.090	0.330
Number of reflections	38400
Completeness [%]	99.4
Redundancy	33

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7.5	293	3.5-4.0 M sodium formate, 50 mM Tris, pH 7.5