5T0S
Synaptotagmin 1 C2B domain, cadmium-bound
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2015-07-07 |
Detector | RIGAKU RAXIS HTC |
Wavelength(s) | 1.54178 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 40.992, 41.948, 80.657 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 36.540 - 1.420 |
R-factor | 0.1624 |
Rwork | 0.159 |
R-free | 0.19820 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1uow |
RMSD bond length | 0.006 |
RMSD bond angle | 1.037 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.10_2155) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.950 | 1.490 |
High resolution limit [Å] | 1.420 | 1.420 |
Rmerge | 0.544 | |
Number of reflections | 26944 | |
<I/σ(I)> | 18.7 | 2.6 |
Completeness [%] | 99.0 | 94.3 |
Redundancy | 4.4 | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 295 | 13.4% PEG 400, 10.05% PEG 1000, 0.15 M potassium phosphate dibasic/sodium phosphate dibasic pH 6.5 |