5T0R
Synaptotagmin 1 C2A domain, cadmium-bound
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2014-12-04 |
Detector | RIGAKU RAXIS HTC |
Wavelength(s) | 1.54178 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 28.064, 63.276, 76.143 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 38.070 - 1.950 |
R-factor | 0.1906 |
Rwork | 0.186 |
R-free | 0.22880 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3f00 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.134 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.10_2155) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.070 | 2.060 |
High resolution limit [Å] | 1.950 | 1.950 |
Rmerge | 0.373 | |
Number of reflections | 10075 | |
<I/σ(I)> | 13 | 3.2 |
Completeness [%] | 96.9 | 85 |
Redundancy | 4.2 | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | 0.01 M tri-sodium citrate, 16% PEG 6000 |