Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU FR-D |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2010-09-03 |
| Detector | RIGAKU RAXIS IV |
| Wavelength(s) | 1.53 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 101.114, 114.231, 175.190 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 20.000 - 1.950 |
| R-factor | 0.1793 |
| Rwork | 0.177 |
| R-free | 0.21590 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1MWV |
| RMSD bond length | 0.023 |
| RMSD bond angle | 1.991 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.8.0151) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 175.190 | 2.060 |
| High resolution limit [Å] | 1.950 | 1.950 |
| Rmerge | 0.473 | |
| Total number of observations | 55548 | |
| Number of reflections | 146277 | |
| <I/σ(I)> | 9.6 | 1.7 |
| Completeness [%] | 98.9 | 97.9 |
| Redundancy | 2.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | 16-20% PEG 4000, 20% MPD, 0.1 M sodium citrate pH 5.6 |
