5SVW
Light-state Structure of Arabidopsis Thaliana Zeitlupe
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CHESS BEAMLINE F1 |
Synchrotron site | CHESS |
Beamline | F1 |
Temperature [K] | 80 |
Detector technology | CCD |
Collection date | 2014-03-06 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 0.9773 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 86.221, 86.221, 200.478 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 41.614 - 2.290 |
R-factor | 0.1691 |
Rwork | 0.166 |
R-free | 0.22780 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3d72 |
RMSD bond length | 0.016 |
RMSD bond angle | 1.645 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.330 |
High resolution limit [Å] | 2.290 | 2.290 |
Rmerge | 0.063 | 0.220 |
Number of reflections | 34852 | |
<I/σ(I)> | 27.6 | 5 |
Completeness [%] | 87.0 | 82.8 |
Redundancy | 2.6 | 2.4 |
CC(1/2) | 0.915 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | 0.1 M Tris ph 8.5, 0.2 M Sodium Acetate trihydrate, 30% w/v PEG 4K |