5OVO
Structure of DraG-GlnZ-delta42-54 complex from Azospirillum brasilense
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | BESSY BEAMLINE 14.1 |
| Synchrotron site | BESSY |
| Beamline | 14.1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2014-02-07 |
| Detector | DECTRIS PILATUS3 S 6M |
| Wavelength(s) | 0.91841 |
| Spacegroup name | H 3 |
| Unit cell lengths | 116.740, 116.740, 105.616 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 45.600 - 1.550 |
| R-factor | 0.14505 |
| Rwork | 0.144 |
| R-free | 0.16453 |
| RMSD bond length | 0.025 |
| RMSD bond angle | 2.443 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 46.800 |
| High resolution limit [Å] | 1.550 |
| Rpim | 0.050 |
| Number of reflections | 77898 |
| <I/σ(I)> | 10.9 |
| Completeness [%] | 99.8 |
| Redundancy | 5.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 298 | 35 % (v/v) glycerol ethoxylate, 0.2 M lithium citrate |
