5OO9
Streptomyces PAC13 (Y55F) with uridine
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-03-22 |
Detector | RIGAKU SATURN A200 |
Wavelength(s) | 1.54178 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 66.604, 66.604, 54.257 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 57.680 - 1.590 |
R-factor | 0.16195 |
Rwork | 0.160 |
R-free | 0.20003 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.005 |
RMSD bond angle | 1.223 |
Data reduction software | XDS |
Data scaling software | Aimless |
Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 57.680 | 1.680 |
High resolution limit [Å] | 1.590 | 1.590 |
Number of reflections | 17643 | 2002 |
<I/σ(I)> | 42.2 | 8.4 |
Completeness [%] | 92.8 | 67.5 |
Redundancy | 3.8 | 1.8 |
CC(1/2) | 0.999 | 0.820 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 293 | 0.1 M MES pH 6.5, 0.2 M NH4SO4, 30 % w/v 5K PEGMME |