5OI9

Trichoplax adhaerens STIL N-terminal domain

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID23-2
Synchrotron site	ESRF
Beamline	ID23-2
Temperature [K]	100
Detector technology	PIXEL
Collection date	2014-03-07
Detector	DECTRIS PILATUS3 2M
Wavelength(s)	0.87292
Spacegroup name	P 1 21 1
Unit cell lengths	66.020, 75.231, 68.530
Unit cell angles	90.00, 97.20, 90.00

Refinement procedure

Resolution	37.615 - 2.090
R-factor	0.1991
Rwork	0.197
R-free	0.24080
Structure solution method	MAD
RMSD bond length	0.003
RMSD bond angle	0.573
Data reduction software	iMOSFLM
Data scaling software	Aimless
Phasing software	CRANK
Refinement software	PHENIX ((1.11.1_2575: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	37.620	2.140
High resolution limit [Å]	2.090	2.090
Rmerge	0.160	0.861
Rpim	0.077	0.416
Number of reflections	39751	3077
<I/σ(I)>	7.8	2
Completeness [%]	100.0	100
Redundancy	5.2	5.2
CC(1/2)	0.993	0.592

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		292	100 mM MES pH 6.0 3 % (v/v) MPD