Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-11-26 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.99998 |
Spacegroup name | P 1 |
Unit cell lengths | 109.070, 109.140, 385.640 |
Unit cell angles | 90.02, 90.01, 59.98 |
Refinement procedure
Resolution | 54.570 - 3.200 |
R-factor | 0.2553 |
Rwork | 0.254 |
R-free | 0.28280 |
Structure solution method | SAD |
RMSD bond length | 0.007 |
RMSD bond angle | 1.074 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 54.570 |
High resolution limit [Å] | 3.200 |
Number of reflections | 251223 |
<I/σ(I)> | 14.83 |
Completeness [%] | 98.9 |
Redundancy | 8.283 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293.15 | 12% PEG 4000 , 500mM Ammonium sulfate, 100mM MES pH=6.0, 1mM DTT |