5O2W
Extended catalytic domain of Hypocrea jecorina LPMO 9A.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-02-20 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 0.872900 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 42.936, 62.125, 48.015 |
Unit cell angles | 90.00, 111.79, 90.00 |
Refinement procedure
Resolution | 44.580 - 2.000 |
R-factor | 0.2021 |
Rwork | 0.200 |
R-free | 0.23820 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.015 |
RMSD bond angle | 1.739 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0071) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.000 | |
High resolution limit [Å] | 2.000 | |
Number of reflections | 21394 | |
<I/σ(I)> | 4.6 | 2 |
Completeness [%] | 94.2 | |
Redundancy | 3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 1.6 M ammonium sulfate and 0.1 M citric acid pH 4.0 |