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5O1J

Lytic transglycosylase in action

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSOLEIL BEAMLINE PROXIMA 1
Synchrotron siteSOLEIL
BeamlinePROXIMA 1
Temperature [K]100
Detector technologyPIXEL
Collection date2016-05-20
DetectorDECTRIS PILATUS 6M
Wavelength(s)1.1
Spacegroup nameP 21 21 21
Unit cell lengths68.135, 69.122, 143.321
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution71.660 - 1.900
R-factor0.2025
Rwork0.201
R-free0.24906
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)4YIM
RMSD bond length0.016
RMSD bond angle1.592
Data reduction softwareXDS
Data scaling softwareXDS
Phasing softwarePHENIX
Refinement softwareREFMAC (5.8.0049)
Data quality characteristics
 Overall
Low resolution limit [Å]71.660
High resolution limit [Å]1.900
Number of reflections54011
<I/σ(I)>7.81
Completeness [%]99.4
Redundancy4.4
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP6.5291.150.2M Zinc acetate, or 0.1 M Sodium cacodylate pH 6.5, 0.1M 18%PEG 8000

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