5NNT

The dimeric structure of LL-37 crystallized in DPC

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALBA BEAMLINE XALOC
Synchrotron site	ALBA
Beamline	XALOC
Temperature [K]	100
Detector technology	PIXEL
Collection date	2013-04-13
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	1
Spacegroup name	P 21 21 21
Unit cell lengths	35.209, 43.703, 54.398
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	29.558 - 2.209
R-factor	0.264
Rwork	0.263
R-free	0.28730
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.003
RMSD bond angle	0.740
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	PHASER
Refinement software	PHENIX ((1.10.1_2155: ???))

Data quality characteristics

	Overall
Low resolution limit [Å]	40.000
High resolution limit [Å]	2.190
Rmeas	0.128
Number of reflections	4568
<I/σ(I)>	8.07
Completeness [%]	98.7
Redundancy	5.9
CC(1/2)	0.999

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		298	30% PEGMME 3350, 100 mM Tris, ph 8