5NLD
Chicken GRIFIN (crystallisation pH: 7.5)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALBA BEAMLINE XALOC |
Synchrotron site | ALBA |
Beamline | XALOC |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-06-13 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9599 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 39.146, 60.736, 53.878 |
Unit cell angles | 90.00, 92.40, 90.00 |
Refinement procedure
Resolution | 39.110 - 0.960 |
R-factor | 0.1374 |
Rwork | 0.137 |
R-free | 0.14940 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | Theoretical model |
RMSD bond length | 0.009 |
RMSD bond angle | 1.489 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX |
Refinement software | PHENIX (1.8.4_1496) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.110 | 0.990 |
High resolution limit [Å] | 0.960 | 0.960 |
Rmerge | 0.023 | 0.300 |
Number of reflections | 148722 | 13666 |
<I/σ(I)> | 15.02 | 2.41 |
Completeness [%] | 97.0 | 89.78 |
Redundancy | 1.9 | 1.7 |
CC(1/2) | 0.820 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 295 | 5% w/v 2-Propanol, 0.1M HEPES pH 7.5 |