5MWD
Crystal structure of the BCL6 BTB-domain with compound 2
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2014-08-21 |
| Detector | DECTRIS PILATUS 6M-F |
| Wavelength(s) | 1.00 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 30.311, 71.761, 54.873 |
| Unit cell angles | 90.00, 105.95, 90.00 |
Refinement procedure
| Resolution | 35.880 - 1.850 |
| R-factor | 0.169 |
| Rwork | 0.167 |
| R-free | 0.20900 |
| RMSD bond length | 0.008 |
| RMSD bond angle | 0.940 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Refinement software | BUSTER (2.11.7) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 35.880 |
| High resolution limit [Å] | 1.850 |
| Number of reflections | 9606 |
| <I/σ(I)> | 12.6 |
| Completeness [%] | 98.8 |
| Redundancy | 3.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 4.5 | 296 | 25 % PEG 3350 15 % Isopropanol 0.2 M Citrate |
