5MVW
Complex between the Leucine Zipper (LZ) and Centrosomin-motif 2 (CM2) domains of Drosophila melanogaster Centrosomin (Cnn)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-12-16 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 1.28229 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 44.880, 44.270, 72.530 |
Unit cell angles | 90.00, 107.77, 90.00 |
Refinement procedure
Resolution | 42.739 - 1.820 |
R-factor | 0.2233 |
Rwork | 0.222 |
R-free | 0.24610 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.005 |
RMSD bond angle | 0.559 |
Data reduction software | xia2 |
Data scaling software | xia2 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 69.070 | 1.870 |
High resolution limit [Å] | 1.820 | 1.820 |
Rmerge | 0.077 | 3.048 |
Rpim | 0.019 | 0.757 |
Number of reflections | 24465 | 1806 |
<I/σ(I)> | 22.9 | 1.1 |
Completeness [%] | 99.5 | 99.8 |
Redundancy | 16.9 | 17 |
CC(1/2) | 1.000 | 0.574 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 294 | 20%(w/v) PEG6K, 0.1M Tris pH8.0, 0.2M MgCl2 |