5LRU
Structure of Cezanne/OTUD7B OTU domain
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID23-1 |
| Synchrotron site | ESRF |
| Beamline | ID23-1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2013-11-28 |
| Detector | DECTRIS PILATUS 6M-F |
| Wavelength(s) | 0.97933 |
| Spacegroup name | P 41 21 2 |
| Unit cell lengths | 103.349, 103.349, 90.199 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 73.079 - 2.200 |
| R-factor | 0.1995 |
| Rwork | 0.198 |
| R-free | 0.21890 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.002 |
| RMSD bond angle | 0.593 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 90.200 | 2.270 |
| High resolution limit [Å] | 2.200 | 2.200 |
| Rmerge | 0.071 | 0.829 |
| Number of reflections | 25409 | |
| <I/σ(I)> | 13.1 | 1.9 |
| Completeness [%] | 100.0 | 99.9 |
| Redundancy | 7.9 | 5.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 291 | 0.1 M Bis-Tris (pH 6.1), 0.2 M magnesium formate |
