5LGG
The N-terminal WD40 domain of Apc1 (Anaphase promoting complex subunit 1)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-11-24 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9795 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 82.633, 113.262, 100.436 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.131 - 2.150 |
R-factor | 0.181 |
Rwork | 0.179 |
R-free | 0.22650 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4ui9 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.198 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (dev_1810) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.131 | 2.223 |
High resolution limit [Å] | 2.150 | 2.150 |
Rmerge | 0.059 | 0.433 |
Number of reflections | 25408 | |
<I/σ(I)> | 16.76 | 2.01 |
Completeness [%] | 97.8 | 84.7 |
Redundancy | 4.8 | 2.5 |
CC(1/2) | 0.999 | 0.891 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5 | 277 | 0.1 M citric acid, pH5.0, 2M NaCl |