5LF8
Human Nucleoside diphosphate-linked moiety X motif 17 (NUDT17)
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I02 |
| Synchrotron site | Diamond |
| Beamline | I02 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2016-02-08 |
| Detector | DECTRIS PILATUS3 6M |
| Wavelength(s) | 0.9900 |
| Spacegroup name | H 3 2 |
| Unit cell lengths | 151.913, 151.913, 81.495 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 75.960 - 2.560 |
| R-factor | 0.23072 |
| Rwork | 0.227 |
| R-free | 0.29823 |
| Structure solution method | SAD |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.617 |
| Data reduction software | xia2 |
| Data scaling software | xia2 |
| Phasing software | autoSHARP |
| Refinement software | REFMAC (5.7) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 75.960 | |
| High resolution limit [Å] | 2.560 | 2.560 |
| Rmerge | 0.067 | |
| Number of reflections | 11806 | |
| <I/σ(I)> | 18 | |
| Completeness [%] | 100.0 | |
| Redundancy | 10.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7 | 277 | 0.1 M SPG pH 7.0 30% PEG1K |
