5LDY

Structure of Yersinia pseudotuberculosis InvD

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06DA
Synchrotron site	SLS
Beamline	X06DA
Temperature [K]	100
Detector technology	PIXEL
Collection date	2014-02-14
Detector	DECTRIS PILATUS 2M-F
Wavelength(s)	1.0000
Spacegroup name	P 43
Unit cell lengths	58.900, 58.900, 274.590
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	44.701 - 2.600
R-factor	0.2331
Rwork	0.230
R-free	0.25300
Structure solution method	SAD
RMSD bond length	0.002
RMSD bond angle	0.470
Data scaling software	XSCALE
Phasing software	PHENIX
Refinement software	PHENIX (1.10_2155)

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	44.701		2.700
High resolution limit [Å]	2.600	10.000	2.600
Rmerge	0.063	0.024	0.416
Number of reflections	28540
<I/σ(I)>	26.62	65.41	5.86
Completeness [%]	99.9	99	99.9
Redundancy	11.3
CC(1/2)	0.999	1.000	0.957

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	8	293	1.9 M ammonium dihydrogen phosphate; 0.1 M TRIS-HCl pH 8.0