5LDV
Crystal Structures of MOMP from Campylobacter jejuni
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID23-1 |
| Synchrotron site | ESRF |
| Beamline | ID23-1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2014-06-27 |
| Detector | DECTRIS PILATUS 6M-F |
| Wavelength(s) | 1.06733 |
| Spacegroup name | P 63 |
| Unit cell lengths | 90.630, 90.630, 104.400 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 39.240 - 2.100 |
| R-factor | 0.19497 |
| Rwork | 0.193 |
| R-free | 0.22241 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.397 |
| Data reduction software | xia2 |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 39.240 | 2.175 |
| High resolution limit [Å] | 2.100 | 2.100 |
| Rmerge | 0.060 | |
| Number of reflections | 28313 | |
| <I/σ(I)> | 29.89 | |
| Completeness [%] | 99.5 | |
| Redundancy | 13.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 4.25 | 295.15 | 0.05M sodium citrate, 35% (v/v) Peg 400, 0.07 M potassium chloride |
