5LCZ
Chimeric GST
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE X13 |
Synchrotron site | EMBL/DESY, HAMBURG |
Beamline | X13 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-10-19 |
Detector | MARRESEARCH |
Wavelength(s) | 0.8081 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 98.920, 91.380, 51.490 |
Unit cell angles | 90.00, 93.18, 90.00 |
Refinement procedure
Resolution | 19.669 - 2.325 |
R-factor | 0.2036 |
Rwork | 0.200 |
R-free | 0.26830 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1pkw |
RMSD bond length | 0.008 |
RMSD bond angle | 1.040 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.390 |
High resolution limit [Å] | 2.320 | 2.320 |
Rmerge | 0.509 | |
Number of reflections | 19517 | |
<I/σ(I)> | 9.04 | 2.3 |
Completeness [%] | 98.5 | 83.4 |
Redundancy | 4.2 | |
CC(1/2) | 0.992 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.4 | 289 | PEG 4000 20% (w/v), ammonium citrate 0.2 M, pH 6.4 |