5L8K
Aurora-A kinase domain in complex with vNAR-D01 (crystal form 2)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-02-13 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 0.91741 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 88.700, 109.720, 45.760 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.660 | 1.840 |
High resolution limit [Å] | 1.790 | 1.790 |
Rmerge | 0.057 | |
Number of reflections | 41932 | |
<I/σ(I)> | 17.7 | 1.2 |
Completeness [%] | 97.8 | 91.4 |
Redundancy | 6.7 | 6.7 |
CC(1/2) | 1.000 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.5 | 295 | 0.2 M ammonium sulfate, 0.1 M bis-Tris pH 5.5, 25 % PEG 3350 |