5L80
Structure of Exuperantia EXO-like and SAM-like domains
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2013-10-27 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 1 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 79.540, 66.590, 81.330 |
| Unit cell angles | 90.00, 113.64, 90.00 |
Refinement procedure
| Resolution | 47.336 - 2.800 |
| R-factor | 0.2535 |
| Rwork | 0.252 |
| R-free | 0.27650 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 5l7z |
| RMSD bond length | 0.003 |
| RMSD bond angle | 0.658 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.900 |
| High resolution limit [Å] | 2.800 | 2.800 |
| Rmerge | 0.078 | 1.045 |
| Number of reflections | 19360 | |
| <I/σ(I)> | 19.4 | 2.2 |
| Completeness [%] | 99.5 | 99.2 |
| Redundancy | 6.7 | 6.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6 | 277 | Sodium Malonate, PEG 1000, MES |
