5KHN
Crystal structures of the Burkholderia multivorans hopanoid transporter HpnN
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-02-27 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.98 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 111.914, 129.546, 111.728 |
Unit cell angles | 90.00, 114.04, 90.00 |
Refinement procedure
Resolution | 93.803 - 3.445 |
R-factor | 0.2848 |
Rwork | 0.283 |
R-free | 0.31900 |
Structure solution method | SIRAS |
RMSD bond length | 0.003 |
RMSD bond angle | 0.604 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHENIX |
Refinement software | PHENIX (1.10.1_2155) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 100.000 | 100.000 | 3.570 |
High resolution limit [Å] | 3.450 | 7.430 | 3.450 |
Rmerge | 0.126 | 0.080 | |
Rmeas | 0.132 | 0.084 | |
Rpim | 0.051 | 0.026 | 0.712 |
Total number of observations | 424764 | ||
Number of reflections | 38588 | ||
<I/σ(I)> | 7.3 | ||
Completeness [%] | 99.9 | 99.9 | 99.9 |
Redundancy | 11 | 11.2 | 10.7 |
CC(1/2) | 0.995 | 0.673 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 3.5 | 298 | 18% PEG2000, and 0.2M LiSo4 |