5K8E
Xylooligosaccharide oxidase from Myceliophthora thermophila C1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | BRUKER AXS MICROSTAR-H |
Temperature [K] | 110 |
Detector technology | IMAGE PLATE |
Collection date | 2015-02-09 |
Detector | MARRESEARCH |
Wavelength(s) | 1.54 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 123.951, 59.440, 68.693 |
Unit cell angles | 90.00, 90.62, 90.00 |
Refinement procedure
Resolution | 53.600 - 1.930 |
R-factor | 0.16056 |
Rwork | 0.159 |
R-free | 0.19544 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ZR6 and 3RJ8 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.327 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 53.600 | 1.970 |
High resolution limit [Å] | 1.930 | 1.930 |
Rmerge | 0.163 | 0.673 |
Number of reflections | 37594 | |
<I/σ(I)> | 11.8 | 2.4 |
Completeness [%] | 99.4 | 91.4 |
Redundancy | 7.2 | 5.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 294 | 15-18% PEG3350, 0.1 M MES buffer, 0.2 M ammonium chloride |