5JVD
Tubulin-TUB092 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-05-19 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.0000 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 104.251, 156.317, 180.614 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.457 - 2.393 |
R-factor | 0.1707 |
Rwork | 0.169 |
R-free | 0.20840 |
RMSD bond length | 0.005 |
RMSD bond angle | 0.873 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.500 | 2.540 |
High resolution limit [Å] | 2.390 | 2.390 |
Rmerge | 2.064 | |
Number of reflections | 116285 | |
<I/σ(I)> | 11.6 | 0.95 |
Completeness [%] | 99.6 | 97.7 |
Redundancy | 7 | 6.97 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 6.7 | 293 | 6% PEG 4K, 4% glycerol, 30 mM MgCl2, 30 mM CaCl2, 100 mM MES/Imidazole |